AR Grade Deuterated Chloroform
Analytical NMR Grade
Analytical Reagent

AR Grade Deuterated Chloroform (CDCl₃)

Ultra-pure Analytical Reagent grade deuterated chloroform specifically manufactured for precision NMR spectroscopy applications. Our AR grade CDCl₃ delivers exceptional deuteration levels and consistent performance for critical analytical work and research applications requiring the highest NMR solvent quality.

  • 99.9% Deuteration Level
  • Analytical Grade Quality
  • Ultra-Low Water Content (≤0.005%)
  • Superior Signal Clarity
  • Analytical Reagent Standard
  • Exceptional Performance
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Technical Specifications

Chemical Name: Deuterated Chloroform
Chemical Formula: CDCl₃
CAS Number: 865-49-6
Molecular Weight: 120.38 g/mol
Deuterium Content: 99.8% D
Physical State: Clear, colorless liquid
Purity: ≥ 99.8% (GC)
Water Content: ≤ 0.01%
Boiling Point: 61.2°C
Density (20°C): 1.500 g/cm³
Refractive Index: 1.4467 (20°C)
Stabilizer: Silver foil
Storage: Store below 25°C, protect from light
Package Sizes: 1mL, 10mL, 100mL ampoules
Shelf Life: 2 years unopened
Grade: Analytical Reagent (A.R.)
¹³C Chemical Shift: 77.16 ppm (reference)
Isotopic Purity: 99.8% deuterated

Applications

¹H NMR Spectroscopy
¹³C NMR Analysis
2D NMR Techniques
Protein NMR Studies
Analytical Chemistry
Academic Research
Pharmaceutical Analysis
Structure Elucidation
Quantitative NMR
Quality Control Testing
Natural Product Analysis
Metabolite Studies

Industry-Specific Grades

DRAVYOM offers specialized deuterated chloroform grades tailored for specific analytical applications, ensuring optimal spectroscopic performance with controlled deuterium content and ultra-low impurities for precise NMR analysis.

NMR Grade
Deuterium: 99.8% D Water: ≤ 0.01% Stabilizer: Silver foil Application: High-resolution NMR
Ultra-Pure Grade
Deuterium: ≥ 99.9% D Water: ≤ 0.005% Purity: ≥ 99.9% Application: Critical NMR studies
Analytical Grade
Deuterium: 99.8% D Purity: ≥ 99.8% Quality: AR specification Application: Routine NMR analysis
Pharmaceutical Grade
Deuterium: 99.8% D Heavy Metals: ≤ 1 ppm Residual Solvents: Controlled Application: Drug analysis

Quality Standards

DRAVYOM's deuterated chloroform is manufactured under stringent quality control protocols, meeting international analytical standards including ACS specifications and NMR-grade requirements for precise spectroscopic analysis.

ISO 9001:2015 Certified Manufacturing
ACS Grade Specifications
99.8% Deuterium Content
Advanced NMR Testing
Ultra-Low Water Content
Temperature Controlled Storage
NMR-Verified Certificate
Inert Atmosphere Packaging

Advanced Chemical Properties & Performance

AR Grade Deuterated Chloroform exhibits exceptional chemical properties essential for analytical applications. Its ultra-pure composition and precise deuteration ensure reliable performance in demanding analytical procedures and research applications.

Analytical Properties
Deuterium Content: 99.8% minimum
Chemical Shift (¹H NMR): δ 7.26 ppm (residual CHCl₃)
Chemical Shift (¹³C NMR): δ 77.0 ppm (triplet)
Relaxation Time T₁: 11.8 seconds
Physical Properties
Boiling Point: 61.2°C
Melting Point: -63.5°C
Density (20°C): 1.500 g/cm³
Refractive Index: 1.4459 (20°C)
Analytical Performance
NMR Resolution: Excellent peak clarity
Signal-to-Noise Ratio: Superior performance
Baseline Stability: Exceptional flatness
Impurity Interference: Minimal spectral noise
Purity Specifications
Total Impurities: ≤ 0.01%
Water Content: ≤ 0.01%
Residual Proton: ≤ 0.2%
Acidity (as HCl): ≤ 0.003%
Stability Properties
Shelf Life: 3 years (unopened)
Light Sensitivity: Protect from light
Temperature Stability: Stable below 25°C
Container Compatibility: Amber glass ampoules

Performance Characteristics

Detailed performance metrics demonstrate AR Grade Deuterated Chloroform superiority in analytical applications with exceptional accuracy, precision, and reproducibility across diverse NMR spectroscopy applications.

NMR Performance

Signal clarity: Superior peak resolution

Exceptional spectral quality
Deuterium Analysis

Deuteration: 99.8% minimum achieved

Ultra-high isotopic purity
Moisture Control

Water content: ≤ 0.01% maintained

Superior moisture exclusion
Temperature Stability

Working range: -10 to 25°C operational

Consistent performance across temperatures
Batch Reproducibility

Variation: ±0.05% between batches

Exceptional lot-to-lot consistency
Ampoule Integrity

Sealed under nitrogen atmosphere

Extended analytical grade integrity

Safety Information

Potentially carcinogenic solvent that requires careful handling. Use only in well-ventilated areas with appropriate protective equipment including chemical-resistant gloves, safety goggles, and lab coats. Avoid skin contact and inhalation of vapors. Ensure emergency procedures are in place.

Carcinogenic
Respiratory Irritant
Eye Irritant

Storage & Handling

Store in original amber glass ampoules in a cool, dry, well-ventilated area away from light and heat sources. Keep ampoules intact until use and protect from moisture. Use in fume hoods with adequate ventilation and ensure proper disposal of waste materials.

Cool storage (2-8°C preferred)
Fume hood operation required
Amber glass ampoules only
Protect from light exposure

Chemical Mechanisms & Reaction Pathways

Deuterated Chloroform exhibits unique isotopic properties through deuterium-hydrogen exchange mechanisms, enabling precise NMR applications with predictable chemical shift patterns and coupling constants for analytical spectroscopy.

Isotopic Exchange

Minimal H-D exchange under normal conditions: CDCl₃ + H₂O ⇌ CHDCl₂ + D₂O

Controlled exchange for NMR stability
Solvent Interactions

Weak van der Waals interactions with solutes for minimal spectral interference

Inert solvent behavior in NMR spectroscopy
Chemical Shifts

Predictable ¹H and ¹³C NMR reference signals for internal standardization

Reliable spectroscopic referencing system
Magnetic Properties

Deuterium nuclear spin-1 effects on spectral resolution and coupling

Enhanced spectral clarity in NMR analysis

Regulatory Compliance & Documentation

Comprehensive regulatory compliance ensures global NMR laboratory access with complete documentation packages supporting international standards and analytical method validations for spectroscopic applications.

ACS Specifications

American Chemical Society NMR grade standards compliance

ISO 6353 Standard

International standard for deuterated solvent specifications

Spectroscopic Grade

NMR spectroscopy grade specifications for analytical applications

REACH Registration

European Union chemical regulation compliance

Method Validation

Supported NMR method validation documentation

SDS Documentation

Multi-language Safety Data Sheets (16 sections, GHS compliant)

Technical Support & Value-Added Services

DRAVYOM's NMR spectroscopy team provides comprehensive method support, troubleshooting assistance, and analytical services to optimize Deuterated Chloroform performance in your specific spectroscopic applications.

Method Development
  • NMR method optimization support
  • Sample preparation guidance
  • Spectral resolution enhancement
  • Custom NMR procedures
Analytical Services
  • Deuteration level verification
  • Water content analysis
  • Impurity profiling
  • NMR performance validation
Technical Support
  • NMR troubleshooting consultation
  • Storage and handling guidance
  • Safety training and protocols
  • Spectroscopy best practices
Supply Solutions
  • Consistent batch scheduling
  • Emergency supply arrangements
  • Custom ampoule sizing
  • Global distribution network

Environmental Impact & Sustainability

Our Deuterated Chloroform production emphasizes environmental responsibility through sustainable manufacturing practices, solvent recovery systems, and comprehensive environmental impact management for NMR laboratory operations.

Solvent Recovery

Advanced deuterated solvent recovery and purification

D₂O Recycling

Deuterium oxide recovery from production processes

Clean Production

Energy-efficient deuteration with emission controls

Safe Disposal

Specialized guidance for deuterated solvent waste

ISO 14001

Environmental management system certified production

Ampoule Recycling

Specialized ampoule return and recycling programs

Manufacturing Excellence & Quality Control

DRAVYOM's specialized deuterated solvent manufacturing facility employs advanced isotopic purification technology and continuous monitoring systems to ensure consistent NMR grade quality and deuteration levels across all production batches.

Deuteration Process

Advanced catalytic deuteration and fractional distillation in controlled atmosphere

Multi-stage isotopic enrichment for NMR grade quality
Isotopic Testing

Mass spectrometry verification of deuteration levels and impurity analysis

NMR performance testing and water content verification
Quality Systems

ISO 9001:2015 quality management with NMR laboratory accreditation

Continuous improvement and method validation
Ampoule Sealing

Flame-sealed amber ampoules with nitrogen atmosphere protection

Moisture exclusion and long-term stability

Market Applications & Performance Data

Comprehensive NMR laboratory data demonstrating Deuterated Chloroform effectiveness across diverse spectroscopic applications with quantified performance metrics and method validations.

NMR Laboratories
Deuteration: ≥99.8% D incorporation Water Content: ≤0.01% maintained Spectral Quality: Superior baseline resolution
Research Institutions
Publication Support: 1000+ NMR methods cited Reproducibility: >99% spectral consistency Innovation: Custom deuteration services
Pharmaceutical NMR
Reliability: 99.9% batch consistency Regulatory: 100% method validation support Efficiency: Enhanced spectral clarity

DRAVYOM Competitive Advantages

Superior Deuteration

Consistently exceeds 99.8% D incorporation with ultra-low protiated solvent contamination

Reliable Supply

Guaranteed availability with strategic inventory management and specialized NMR solvent production

NMR Expertise

Dedicated NMR spectroscopy team provides method development and troubleshooting support

Quality Assurance

Traceable certificates with comprehensive isotopic data and NMR performance validation

Global Standards

International compliance with NMR grade specifications for worldwide acceptance

Partnership Approach

Collaborative relationships with NMR facilities and custom deuteration services